Microscale and miniscale organic chemistry laboratory experiments ebook

Other Editions 1. Friend Reviews. To see what your friends thought of this book, please sign up. To ask other readers questions about Microscale and Miniscale Organic Chemistry Laboratory Experiments , please sign up. Lists with This Book. Community Reviews. Showing Average rating 3. Rating details. More filters. Sort order. Jun 06, Lou Rocama marked it as reference Shelves: all-non-fiction , p-read-for-school , xa-s , y-read , y-read , nsc-chemistry-and-physics , ns-science , ns-practical , xx , p-x.

We didn't go through every experiment in this thank god , so I can only generalize from what I did use. It covers concepts differently than our lecture text, and has quite a lot that weren't covered in that book at all, which was nice.

The procedures are pretty easy to follow, and seemed to work well when we followed them. That last is the trick, though. Often our instructor adjusted reagent amounts to give better yields, or to reduce time spent in synthesis. Occasionally the other lab section wo We didn't go through every experiment in this thank god , so I can only generalize from what I did use.

Occasionally the other lab section would benefit from this, as amounts were tweaked further after my class ended up with uniformly poor yields. Evaporations are always done with an erlenmeyer flask in this book. This is a wonderful idea, if you have a spare two hours. We learned to ignore these specifications, and use beakers instead. Of course, UCCS has nice hoods, and if you're in the open, you might have to suffer the longer wait.

On the other hand, why are you evaporating poisons in the open at all? My biggest difficulty with this was the critical thinking questions. They're interesting and pertinent questions, I'll grant, but they aren't answered anywhere. The answers aren't indicated in the text at all in most experiments, leading most to that compulsive liar, the internet. Even the internet failed in a couple of cases. They did induce critical thinking, but most of that thinking was the wrong sort of critical.

The safety sections are pathetic. If you want to know safety information, use hazard. If you don't want to know safety information, do it anyway. There're some nasty reagents used in this, and there's no guarantee you won't get exposed to them. It's not bad, but does require a very available and on the ball instructor to use. On the upside, this might be the only text that doesn't come out with a new edition every year.

The current edition is ten years old. This makes it pretty easy to find used. Also, considering the author teaches at my university, any new edition might use the aforementioned tweakings undergraduates make good labrats, after all. The third part consists of a collection of 84 experiments, divided into 5 modules and arranged according to complexity. The last two chapters are devoted to the practices at Microscale Synthesis and Green Chemistry, seeking alternatives to traditional Organic Chemistry.

Organizes lab course coverage in a logical and useful way Features a valuable chapter on Green Chemistry Experiments Includes 84 experiments arranged according to increasing complexity. All sections have been updated to reflect new techniques, equipment and technologies, and the text has been revised with an even sharper focus on practical skills and procedures. The first half of the book is devoted to safe laboratory practice as well as purification and analytical techniques; particularly spectroscopic analysis.

The second half contains step-by-step experimental procedures, each one illustrating a basic principle, or important reaction type. Tried and tested over almost three decades, over validated experiments are graded according to their complexity and all are chosen to highlight important chemical transformations and to teach key experimental skills.

New sections cover updated health and safety guidelines, additional spectroscopic techniques, electronic notebooks and record keeping, and techniques, such as semi-automated chromatography and enabling technologies such as the use of microwave and flow chemistry.

New experiments include transition metal-catalysed cross-coupling, organocatalysis, asymmetric synthesis, flow chemistry, and microwave-assisted synthesis.

Author : Daniel R. Cutting-edge subjects such as HPLC, bioorganic chemistry, multistep synthesis, and more are presented in a clear and engaging fashion. Author : Clark F. Material is organized in four sections: techniques, experiments, organic qualitative analysis, and appendixes. The experiments section moves on to more. Primarily intended for the undergraduate students of science, the book deals with the practical aspects of organic chemistry and discusses how experiments should be done in the laboratory.

The book introduces the various types of components used in laboratories and describes basic techniques used for purification. It elaborates different methods of identification of organic compounds, their preparation, and analysis. In addition, it emphasizes qualitative analysis of organic compounds. The book contains essential experiments done in an organic lab and also. Home » Books » Experimental Organic Chemistry.

Previous edition by Laurence M. Author : Philippa B. Dobado,Henar Martnez-garca,Francisco G. Author : John C. Gilbert,Stephen F. Author : Charles F. Wilcox,Mary F.